10.22376/ijpbs.2019.10.1.p1-12 Volume 7 Issue 1 2016 (January - March) lessThan i greaterThan Citrus grandis lessThan /i greaterThan commonly known as pomelo, shaddock or limau bali belongs to the family Rutaceae. The aim of this study is to identify the phytochemical components present in white flesh lessThan i greaterThan C. grandis lessThan /i greaterThan fruit peels using solvent extraction and hydro distillation methods. Identification of phytochemical compounds was conducted using the GC-MS analysis and Nuclear Magnetic Resonance (NMR) spectroscopic techniques. Hexadecanoic acid and 9,12-Octadecadienoic acid (Z,Z) are 2 major compounds elucidated from hexane and ethyl acetate fractions, respectively; while limonene was identified as a major compound in essential oil. White powder obtained during methanol extraction was confirmed as naringin using NMR spectroscopic technique. M. S. MANORENJITHA, J. ZAIRI, S.K. LING, J. MAILINA AND H. NUZIAH Citrus grandis, naringin, hexadecanoic acid, 9,12-Octadecadienoic acid (Z,Z), limonene 267-278